HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Amino-2,3-dihydro-1H-indene-1-carboxylic acid → HCID 45254375, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Amino-2,3-dihydro-1H-indene-1-carboxylic acid | HCID 233810 | — |
| Reactant | 2,6-Dichloroquinoline-3-carboxylic acid | HCID 24266068 | — |
| Product | HCID 45254375 | HCID 45254375 | 8% |
Reaction Steps
In close analogy to the procedure described in Example 1, 2,6-dichloroquinoline-3-carboxylic acid is reacted with DL-1-aminoindan-1-carboxylic acid to provide the title compound in 8% yield as yellow needles (flash chromatography on SiO2, eluent CHCl3, MeOH, AcOH—15, 1, 0.2 and recrystallization from MeOH).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08288549B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-5c1712e5b0c946a99ac30961eb8672e9 |
| Source note | uspto-grants-2012_10 |