HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloronicotinic acid → HCID 45256527, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloronicotinic acid | HCID 76258 | — |
| Reactant | HCID 67357599 | HCID 67357599 | — |
| Product | HCID 45256527 | HCID 45256527 | — |
Reaction Steps
In close analogy to the procedure described in Example 96, 2-[1-carboxy-2-(4-hydroxy-phenyl)-ethylamino]-6-chloro-quinoline-3-carboxylic acid is reacted with 2-chloronicotinic acid to provide the title compound in a form of diammonia salt after chromatography on silica (aq. ammonia containing eluent).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08288549B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-20035e22d20d4ab4a054b81341eaff71 |
| Source note | uspto-grants-2012_10 |