HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nicotinic Acid → HCID 59392506, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nicotinic Acid | HCID 938 | — |
| Reactant | Tert-butyl 6-chloropyridine-3-carboxylate | HCID 11521348 | — |
| Reactant | HCID 178418529 | HCID 178418529 | — |
| Product | HCID 59392506 | HCID 59392506 | — |
Reaction Steps
6-(3-Methyl-butyl)-nicotinic acid is prepared by reacting 6-chloro-nicotinic acid tert-butly ester with 3-methyl-butylmagnesium bromide under Fürstner conditions as described for Nicotinic acid 2; LC-MS: tR=0.58 min, [M+1]+=194.30.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08288554B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-07f4f4bd9d8648e984c98830aca3c4e5 |
| Source note | uspto-grants-2012_10 |