Cupric acetate monohydrate → Cupric acetate

Temperature

60 °C

Tablet also lists the important synthesis parameters for the ion-exchange in the preparation of example 6. A copper acetate solution was prepared by dissolving 57.5 g copper acetate monohydrate in 2822.5 g deionized water in a jacketed 4 Liter glass reactor. This solution was heated to 60° C. before addition of 360 g of the Na-CHA (example 1B). 150 g of deionized water was used to wash the reactor walls to insure all zeolite was in solution. The volume of the exchange slurry was kept constant at a liquid:solid ratio of 8:1. The temperature of 60° C. was maintained for 8 hours during which the pH ranged from 4.75 to 4.5. After 8 hours of ion-exchange the slurry was filtered hot over a 33 cm diameter Buechner funnel using 541 Whatmann filter paper (>25 μm filtration). The filtercake was then washed with deionized water until the conductivity of the washwater reached 200 μScm−1. The sample was washed with room temperature washwater. The resulting powder was then dried in an oven at 120° C. for 16 hours.

1. customthe important synthesis parameters for the ion-exchange
2. customin the preparation of example 6
3. washto wash the reactor walls
4. filtrationAfter 8 hours of ion-exchange the slurry was filtered hot over a 33 cm diameter Buechner funnel
5. filtrationfilter
6. filtrationpaper (>25 μm filtration)
7. washThe filtercake was then washed with deionized water until the conductivity of the washwater
8. washThe sample was washed with room temperature washwater
9. customThe resulting powder was then dried in an oven at 120° C. for 16 hours

ORD record

ord-39ba9ca8eed64857ac6736e5d9fa51a6

Source dataset

uspto-grants-2012_10

DOI

10.6084/m9.figshare.5104873.v1

Patent number

US08293198B2