Cyclopentanol → Phenol, 3-(cyclopentyloxy)-

HRID 2066379Notes

Reaction equation

[C:1]([O:9][C:10]1[CH:15]=[CH:14][CH:13]=[C:12]([OH:16])[CH:11]=1)(=O)[C:2]1[CH:7]=[CH:6][CH:5]=CC=1.C1(O)CCCC1>>[CH:1]1([O:9][C:10]2[CH:11]=[C:12]([OH:16])[CH:13]=[CH:14][CH:15]=2)[CH2:2][CH2:7][CH2:6][CH2:5]1

Participants

Reactant 2

HCID 7298Cyclopentanol

HCID 8690Resorcinol, monobenzoate

Product 1

HCID 11252318Phenol, 3-(cyclopentyloxy)-Yield 120.2%

Procedure

By using 3-hydroxyphenyl benzoate (50 mg) and cyclopentanol (23.5 μl) as starting materials, the title compound (50 mg) was obtained in the same manner as that of Reference Example 15.

Sources & evidence

ORD record: ord-013dad5fe20447e58544a815c4782748
Source dataset: uspto-grants-2012_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08293715B2

Reaction notes

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