HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66851478, compound → HCID 66890967, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66851478 | HCID 66851478 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 66890967 | HCID 66890967 | — |
Reaction Steps
The title compound was prepared in analogy to the procedure described in Step 1.8 but (2S,3S)-3-(acetylamino-methyl)-1-((S)-1-phenyl-ethyl)-pyrrolidine-2-carboxylic acid amide (Step 5.2) was used instead of (2S,3R)-3-methyl-1-((S)-1-phenyl-ethyl)-pyrrolidine-2-carboxylic acid amide. Moreover, 10% Pd on charcoal, wet with 50% H2O (Aldrich 330108) was used instead of the dry catalyst.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08293753B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-64498bd18a5c48b58ad0a7b3a213c2f1 |
| Source note | uspto-grants-2012_10 |