HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58092731, compound → HCID 58092709, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58092731 | HCID 58092731 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 58092709 | HCID 58092709 | — |
Reaction Steps
The title compound was prepared in analogy to the procedure described in Step 1.8 but (2S,3S)-3-morpholin-4-ylmethyl-1-((S)-1-phenyl-ethyl)-pyrrolidine-2-carboxylic acid amide (Step 7.2) was used instead of (2S,3R)-3-methyl-1-((S)-1-phenyl-ethyl)-pyrrolidine-2-carboxylic acid amide. Moreover, 10% Pd on charcoal, wet with 50% H2O (Aldrich 330108) was used instead of the dry catalyst.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08293753B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-9df93ac5037e455dbd2f129d5ff13e1a |
| Source note | uspto-grants-2012_10 |