HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1'-Carbonyldiimidazole → HCID 86649580, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | HCID 58095737 | HCID 58095737 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86649580 | HCID 86649580 | — |
Reaction Steps
CDI (0.10 g) was added to a stirred solution of 5-[2-(1-fluoro-1-methyl-ethyl)-pyrimidin-4-yl]-4-methyl-thiazol-2-ylamine (Step 9.2) (0.15 g) in CH2Cl2 (4 mL) at rt. The reaction mixture was then stood for 56 h at 25° C. and the title compound isolated by filtration.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08293753B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-6cf9ffbf96b74d2c8a40dd24af6e097f |
| Source note | uspto-grants-2012_10 |