Triphenylphosphine → HCID 58092761, compound

Participants

Reaction Steps

A mixture of (2S,3S)-3-azidomethyl-1-((S)-1-phenyl-ethyl)-pyrrolidine-2-carboxylic acid amide (Step 5.3) (0.723 mmol) and triphenylphosphine (0.867 mmol) in THF (3 mL) was stirred at it for 25 h. The reaction mixture was concentrated to afford the crude title compound as a light brown solid. HPLC: tR 3.53 min (method B); ESI-MS: [M+H]+ 248.

Provenance & Evidence