HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclobutyl 4-nitrophenyl carbonate → HCID 58333505, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclobutyl 4-nitrophenyl carbonate | HCID 22708352 | — |
| Reactant | 1-(2-Fluoro-4-methanesulfonyl-phenyl)-piperidin-4-one O-piperidin-4-yl-oxime | HCID 86655022 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 58333505 | HCID 58333505 | — |
Reaction Steps
To the reaction mixture of 64a obtained above was added 63a (30 mg, 0.08 mmol) in 0.3 mL of DCM. The mixture was stirred at room temperature for 2 h, concentrated and purified on preparative HPLC to give 64-1: LC-MS 468.4 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08293729B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-dc13bcc3bd574d0098be753dc1d91163 |
| Source note | uspto-grants-2012_10 |