HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 58677657, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Water ethylacetate | HCID 22728543 | — |
| Reactant | HCID 67314552 | HCID 67314552 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 58677657 | HCID 58677657 | — |
Reaction Steps
A solution of compound 406 (426 mg, 0.94 mmol) and K2CO3 (195 mg, 1.41 mmol) in methanol (4.0 mL) were stirred at RT for 5 h. The reaction mixture was poured into a mixture of EtOAc/water. The organic phase was washed with water, brine and then dried (MgSO4), filtered and concentrated in vacuo to give the crude title compound. The product was used without any further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08293772B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-eb3c9c38724444e588cf6e4b06ea2a11 |
| Source note | uspto-grants-2012_10 |