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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2067191Generated: October 31, 2026

Potassium Carbonate → HCID 58677657, compound

https://huagongshe.com/reaction/2067191

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
ReactantWater ethylacetateHCID 22728543—
ReactantHCID 67314552HCID 67314552—
SolventMethanolHCID 887—
ProductHCID 58677657HCID 58677657—

Reaction Steps

A solution of compound 406 (426 mg, 0.94 mmol) and K2CO3 (195 mg, 1.41 mmol) in methanol (4.0 mL) were stirred at RT for 5 h. The reaction mixture was poured into a mixture of EtOAc/water. The organic phase was washed with water, brine and then dried (MgSO4), filtered and concentrated in vacuo to give the crude title compound. The product was used without any further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08293772B2
Source datasetuspto-grants-2012_10
ORD IDord-eb3c9c38724444e588cf6e4b06ea2a11
Source noteuspto-grants-2012_10