HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-azido-acetamide → HCID 86605522, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-azido-acetamide | HCID 3246223 | — |
| Reactant | 3-Chloropropane-1-sulfonamide | HCID 13614818 | — |
| Product | HCID 86605522 | HCID 86605522 | — |
Reaction Steps
The reaction was carried out similarly as described in the preparation of compound 411, using compound 3-chloro-propane-1-sulfonic acid amide (19.0 mmol). The crude product was purified by continuous gradient flash chromatography using EtOAc/petroleum ether (40-60) 35:65 to 65:35 as the eluent to afford the title compound as colourless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08293772B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-60ba2f2e123d4fbaa3beccc533e74e73 |
| Source note | uspto-grants-2012_10 |