HRID2067226

反应详情

EQUATION

反应方程式

HRID 2067226 的结构方程式

PROCEDURE

实验过程

The reaction was carried out similarly as described in the preparation of compound 406, using compound 430 (7.17 mmol) and ethynyltrimethylsilane (7.17 mmol). The crude product was purified by flash chromatography using EtOAc/petroleum ether (40-60) 1:8 as the eluent to afford the title compound as yellow solid.

WORKUP

后处理

  1. customThe crude product was purified by flash chromatography