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HRID2067763

反应详情

EQUATION

反应方程式

HRID 2067763 的结构方程式

REACTANTS

反应物

3
结构：Br.CN(C)CCBr
HCID45791347

2-Bromo-N,N-dimethylethan-1-amine--hydrogen bromide (1/1)

C4H11Br2N

结构：Cn1c(=O)cc(Nc2ccc(I)cc2F)c2c(=O)n(C[C@H]3COC(C)(C)O3)cnc21
HCID59823036

未命名化合物

结构：Cn1c(=O)cc(Nc2ccc(N)cc2F)c2c(=O)[nH]cnc21
HCID135741654

未命名化合物

PRODUCTS

生成物

1
结构：CN(C)CCn1cnc2c(c(Nc3ccc(I)cc3F)cc(=O)n2C)c1=O
HCID24967884

未命名化合物

PROCEDURE

实验过程

The title compound was prepared following the same procedure for the synthesis of compound 5G using compound 5F and 2-bromo-N,N-dimethylethanamine hydrobromide as starting material. 1H NMR (400 MHz, MeOD) δ 8.57 (s, 1 H) 7.68 (m, 2H) 7.33 (t, J=8.36 Hz, 1 H) 5.78 (s, 1 H) 4.51 (t, J=4.0 Hz, 2 H) 3.69 (s, 3 H) 3.66 (t, J=8.0 Hz, 2 H) 3.09 (s, 6 H). [M+H] calc'd for C18H19FIN5O2, 484; found, 484.