HRID2068164

反应详情

EQUATION

反应方程式

HRID 2068164 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

CONDITIONS

反应条件

温度
30 °C

PROCEDURE

实验过程

A mixture of 10.02 g of 200 proof ethanol and 0.502 g of 98% sodium succinate was prepared and heated to 30° C. These quantities allowed for a final solution of 10 wt % succinic acid in ethanol to be obtained upon acidification. The solubility of succinic acid in ethanol at 30° C. is about 12 wt %. Sulfuric acid (H2SO4) (0.338 g, 98%) was added to the ethanol/sodium succinate slurry with stirring to produce free succinic acid and sodium sulfate.

WORKUP

后处理

  1. customwas prepared
  2. customto be obtained upon acidification
  3. customat 30° C.