Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Sodium Succinate | HCID 9020 | — |
| Reactant | Ethanol sodium succinate | HCID 86659235 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Succinic Acid | HCID 1110 | — |
| Product | Sodium Sulfate | HCID 24436 | — |
Reaction Steps
A mixture of 31.83 g of 200 proof ethanol and 4.356 g of 98% sodium succinate was prepared and heated to 30° C. Sulfuric acid (2.817 g, 98%) was then added to the ethanol/sodium succinate slurry with stiffing to produce free succinic acid and sodium sulfate. Following the procedure described in Example 1, a conversion of 68.6% of sodium succinate was obtained after 1 hour.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08293935B2 |
|---|
| Source dataset | uspto-grants-2012_10 |
|---|
| ORD ID | ord-84e6baccd88d4d4ab26f9652883300c9 |
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| Source note | uspto-grants-2012_10 |
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