Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 67253031 | HCID 67253031 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 24798638 | HCID 24798638 | — |
Reaction Steps
A mixture of (2-(5-(4-methoxypyridin-3-yl)-1-((2-(trimethylsilyl)ethoxy)methyl)-1H-indazol-3-ylamino)-1-phenyl-1H-benzo[d]imidazol-5-yl)methanol (0.024 g, 0.000040 mol) and 0.03 M HCl (1 mL,) in ethanol (3 mL) was heated at 100° C. for 2 hours. The reaction was concentrated and the residue was dissolved in DMSO and purified by HPLC.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08293923B2 |
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| Source dataset | uspto-grants-2012_10 |
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| ORD ID | ord-d8650f12f42c4870bf6db31f75cfadbc |
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| Source note | uspto-grants-2012_10 |
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