Methyl Salicylate → HCID 67549718, compound

HRID 2068471Notes

Reaction equation

[C:1]([O:10][CH3:11])(=[O:9])[C:2]1[C:3](=[CH:5][CH:6]=[CH:7][CH:8]=1)O.C(O)[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH3:23].[CH3:25][O:26][C:27]([C:29]1[CH:30]=[CH:31]C(O)=[CH:33][CH:34]=1)=[O:28].C(C(CCCCCC)CO)CCC>>[C:1]([O:10][C:11]1[CH:31]=[CH:30][C:29]([C:27]([O:26][CH2:25][CH:17]([CH2:16][CH2:15][CH2:14][CH3:13])[CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH3:23])=[O:28])=[CH:34][CH:33]=1)(=[O:9])[C:2]1[CH:3]=[CH:5][CH:6]=[CH:7][CH:8]=1

Participants

Reactant 4

HCID 4133Methyl Salicylate

HCID 7456Methylparaben

HCID 81931-Dodecanol

HCID 198002-Butyl-1-octanol

Product 1

HCID 67549718HCID 67549718, compoundYield 71.2%

Procedure

In place of 25 g of methyl salicylate and 31 g of n-dodecanol in Example 1-6, 25 g of methyl p-hydroxybenzoate and 31 g of 2-butyl octanol were used for preparation in the same manner in Example 1-6 to obtain 48 g of 2-butyloctyl p-benzoyloxybenzoate.

Sources & evidence

ORD record: ord-1347934844f946c0bc0508a7ac74f8af
Source dataset: uspto-grants-2012_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08299004B2

Reaction notes

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