HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylimidazole → HCID 11682363, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylimidazole | HCID 12749 | — |
| Reactant | N-(6-fluoro-7-nitro-2,4-dioxo-1,4-dihydro-2H-quinazolin-3-yl)-methanesulfonamide | HCID 58964482 | — |
| Product | HCID 11682363 | HCID 11682363 | 49% |
Reaction Steps
N-(6-Fluoro-7-nitro-2,4-dioxo-1,4-dihydro-2H-quinazolin-3-yl)-methanesulfonamide (25 mg, 0.0786 mmol) is reacted with 2-methyl-1H-imidazole according to the GPA affording 14.5 mg (49%) of a yellowish powder. Rt=1.98 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08299085B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-fb0308e3abcc47a0b30983a74298542f |
| Source note | uspto-grants-2012_10 |