HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(6-fluoro-7-nitro-2,4-dioxo-1,4-dihydro-2H-quinazolin-3-yl)-methanesulfonamide → HCID 11717840, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(6-fluoro-7-nitro-2,4-dioxo-1,4-dihydro-2H-quinazolin-3-yl)-methanesulfonamide | HCID 58964482 | — |
| Reactant | HCID 178418800 | HCID 178418800 | — |
| Product | HCID 11717840 | HCID 11717840 | 43% |
Reaction Steps
N-(6-Fluoro-7-nitro-2,4-dioxo-1,4-dihydro-2H-quinazolin-3-yl)-methanesulfonamide (25 mg, 0.0786 mmol) is reacted with 4-methyl-1H-imidazole according to the GPB affording 12.6 mg (43%) of a yellowish powder as a 5 to 1 regioisomer mixture. Rt=2.11 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08299085B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-130d209d6760491490bff4b0533878e7 |
| Source note | uspto-grants-2012_10 |