HuagongsheHuagongshe Chemistry Print Report · For research reference only
Valinol → HCID 69450639, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Valinol | HCID 79019 | — |
| Reactant | N-(6-fluoro-7-nitro-2,4-dioxo-1,4-dihydro-2H-quinazolin-3-yl)-methanesulfonamide | HCID 58964482 | — |
| Product | HCID 69450639 | HCID 69450639 | 45% |
Reaction Steps
N-(6-Fluoro-7-nitro-2,4-dioxo-1,4-dihydro-2H-quinazolin-3-yl)-methanesulfonamide (30 mg, 0.0943 mmol) is reacted with 2-amino-3-methyl-butan-1-ol according to the GPA affording 17 mg (45%) of a red powder. Rt=4.00 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08299085B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-e4e76837994144ffbf55d7e048f760ce |
| Source note | uspto-grants-2012_10 |