HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53977558, compound → HCID 69338360, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53977558 | HCID 53977558 | — |
| Reactant | N-(6-fluoro-7-nitro-2,4-dioxo-1,4-dihydro-2H-quinazolin-3-yl)-methanesulfonamide | HCID 58964482 | — |
| Product | HCID 69338360 | HCID 69338360 | 53% |
Reaction Steps
N-(6-Fluoro-7-nitro-2,4-dioxo-1,4-dihydro-2H-quinazolin-3-yl)-methanesulfonamide (30 mg, 0.0943 mmol) is reacted with (R)-2-amino-2-(3,4-dimethoxy-phenyl)-ethanol according to the GPA affording 24.8 mg (53%) of a red powder. Rt=3.80 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08299085B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-03a31fe1b1334585b13c811953810593 |
| Source note | uspto-grants-2012_10 |