HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 87545137, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 59149677 | HCID 59149677 | — |
| Product | HCID 87545137 | HCID 87545137 | — |
Reaction Steps
200 mg (0.78 mmol) of trans-2-[6-(4-fluoro-phenyl)-pyridin-3-yl]-cyclopropanecarboxylic acid were dissolved in 5 ml of thionyl chloride and heated under reflux for 3 h. The mixture was evaporated to dryness. The residual oil was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08299102B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-9b78aa2f0c014d7ebe1783e0f0317765 |
| Source note | uspto-grants-2012_10 |