HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylhydrazine → HCID 68708522, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylhydrazine | HCID 7516 | — |
| Reactant | 3-Oxabicyclo(3.1.0)hexane-2,4-dione | HCID 2734721 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 68708522 | HCID 68708522 | — |
Reaction Steps
1.2 g (11.1 mmol) of phenylhydrazine was dissolved in 20 ml of dichloromethane and 1.24 g (11.1 mmol) of 3-oxa-bicyclo[3.1.0]hexane-2,4-dione were added. The resulting solution was stirred at room temperature for 16 h. The precipitated product was isolated by filtration and washed with dichloromethane. Yield: 1.85 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08299102B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-5e527090b4c14bf998dfdcd615e0cd5c |
| Source note | uspto-grants-2012_10 |