HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydroxy-2-methylbenzonitrile → HCID 178429063, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydroxy-2-methylbenzonitrile | HCID 308741 | — |
| Reactant | HCID 178426655 | HCID 178426655 | — |
| Product | HCID 178429063 | HCID 178429063 | — |
Reaction Steps
The title compound is obtained as a beige oil (0.65 g) in analogy to rac-4-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-N-hydroxy-3,5-dimethyl-benzamidine starting from 4-hydroxy-2-methyl-benzonitrile and L-alpha-beta-isopropyliden glycerol; LC-MS: tR=0.62 min, [M+H]+=281.0.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08299086B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-c432269e2c2d407a9cfa76c2ddac0d01 |
| Source note | uspto-grants-2012_10 |