HRID2070032
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
1-(3-Fluoropropyl)-4-nitro-2-(trifluoromethyl)benzene (300 mg, 1.8 mmol) was dissolved in methanol (10 mL), and palladium carbon (10%, 60 mg) was added thereto. The resulting mixture was stirred under hydrogen atmosphere at room temperature for 3 hours. The catalyst was removed by filtration to give 4-(3-fluoropropyl)-3-(trifluoromethyl)aniline (247 mg, 93%) as a light-yellow oil.
WORKUP
后处理
- customThe catalyst was removed by filtration