HCID 2755516, compound → HCID 14520121, compound

Participants

Reaction Steps

A mixture of 4-[(methyloxy)methyl]-2-nitrophenol D55 (0.72 g, 3.93 mmol) and platinum (IV) oxide (0.089 g, 0.393 mmol) in ethanol (15 mL) was stirred under an atmosphere of hydrogen for 16 hr. The catalyst was removed by filtration through celite and the filtrate concentrated to dryness in vacuo to afford the title compound as a green/brown solid 0.51 g, 85%.

Provenance & Evidence