HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Acetate → HCID 24849296, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Acetate | HCID 517044 | — |
| Reactant | 8-(4-bromobutoxy)-4-(3,5-dichloropyridin-4-ylamino)-7-methoxy-2H-chromen-2-one | HCID 24849567 | — |
| Product | HCID 24849296 | HCID 24849296 | — |
Reaction Steps
The title compound can be prepared from potassium acetate and 8-(4-bromobutoxy)-4-(3,5-dichloropyridin-4-ylamino)-7-methoxy-2H-chromen-2-one (Example 25) following the procedure outlined in Example 52. 1H NMR (400 MHz, CD3OD): δ 8.70 (s, 2H), 7.84 (d, 1H), 7.16 (d, 1H), 4.77 (s, 1H), 4.16 (t, 2H), 4.11 (t, 2H), 3.98 (s, 3H), 2.02 (s, 3H), 1.91 (m, 2H), 1.84 (m, 2H); MS (ESI): 466.9.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07745646B2 |
| Source dataset | uspto-grants-2010_06 |
| ORD ID | ord-a20790e18be94667a8d9e99f9f95ce8c |
| Source note | uspto-grants-2010_06 |