HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 87536207, compound → (1H-Indol-7-YL)methanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 87536207 | HCID 87536207 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | (1H-Indol-7-YL)methanamine | HCID 21950026 | — |
Reaction Steps
(Z)-1H-indole-7-carbaldehyde oxime (100 mg, 0.60 mmol) in MeOH (5 mL), Pd(OH)2 (50 mg) was added and stirred under hydrogen atmosphere (balloon pressure) for 4 h. Reaction mixture was then filtered and solvent evaporated to yield (1H-indol-7-yl)methanamine in quantitative yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08299267B2 |
| Source dataset | uspto-grants-2012_10 |
| ORD ID | ord-9a620c84e1084ad08c247bf65c816272 |
| Source note | uspto-grants-2012_10 |