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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2071038Generated: November 1, 2026

HCID 68670292, compound → HCID 59569980, compound

https://huagongshe.com/reaction/2071038

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 68670292HCID 68670292—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
SolventEthyl AcetateHCID 8857—
ProductHCID 59569980HCID 59569980—

Reaction Steps

A mixture of about 92 mg of crude methyl 3-(aminomethyl)-5-(prop-1-en-2-yl)phenylcarbamate and 17.6 mg of 10% Pd/C in 7 mL of MeOH and 2 mL of EtOAc was stirred at r.t. under H2 balloon for 16 h. The mixture was filtered through Celite and concentrated to give the amine product which was used without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08299267B2
Source datasetuspto-grants-2012_10
ORD IDord-9a506bc2cf09482c946527c2ca058f21
Source noteuspto-grants-2012_10