2,4-Dichloro-1,3-dinitro-5-(trifluoromethyl)benzene → HCID 21413101, compound

HRID 2071239Notes

Reaction equation

HRID 2071239 reaction equation
[CH2:1]([NH2:4])[C:2]#[CH:3].[Cl:5][C:6]1[C:11]([N+:12]([O-:14])=[O:13])=[C:10](Cl)[C:9]([N+:16]([O-:18])=[O:17])=[CH:8][C:7]=1[C:19]([F:22])([F:21])[F:20]>C1CCCCC1>[C:1]([NH:4][C:10]1[C:9]([N+:16]([O-:18])=[O:17])=[CH:8][C:7]([C:19]([F:20])([F:21])[F:22])=[C:6]([Cl:5])[C:11]=1[N+:12]([O-:14])=[O:13])#[C:2][CH3:3]

Participants

4

Reactant 2

HCID 943982,4-Dichloro-1,3-dinitro-5-(trifluoromethyl)benzeneHCID 239041Propargylamine

Product 1

HCID 21413101HCID 21413101, compound

Reagents, catalysts & solvents 1

HCID 8078CyclohexaneSolvent

Procedure

The compound was prepared by reacting propargylamine with 2,4-dichloro-3,5-dinitrobenzotrifluoride in cyclohexane to give the product melting at 86°-87° C.

Workup

  1. customThe compound was prepared

Sources & evidence

ORD record
ord-3b18ef0c455340abb41fa4897dae820e
Source dataset
uspto-grants-1977_09
Patent number
US04046758

Reaction notes

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