HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isothiocyanatotrimethylsilane → HCID 21413759, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isothiocyanatotrimethylsilane | HCID 75297 | — |
| Reactant | Phenanthridine, 1,2,3,4,7,8,9,10-octahydro-6-methyl- | HCID 11298606 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Product | HCID 21413759 | HCID 21413759 | — |
Reaction Steps
By the method of Example 2, 1,2,3,4,7,8,9,10-octahydro-6-methyl-phenanthridine is reacted with n-butyl-lithium solution and the resulting anion is reacted with trimethylsilyl isothiocyanate to give 1,2,3,4,7,8,9,10-octahydro-6-methylphenanthridine-4-thiocarboxamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04046895 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-66812808f29d49579c398d7b84bfc254 |
| Source note | uspto-grants-1977_09 |