HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12794151, compound → HCID 178506822, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12794151 | HCID 12794151 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Product | HCID 178506822 | HCID 178506822 | — |
Reaction Steps
By the method of Example 2, 1,2,3,4,7,8,9,10-octahydro-6-phenyl-phenanthridine is reacted with n-butyl-lithium solution to give 1,2,3,4,7,8,9,10-octahydro-4-lithio-6-phenylphenanthridine which in turn is reacted with trimethylsilyl isothiocyanate to give 1,2,3,4,7,8,9,10-octahydro-6-phenylphenanthridine-4-thiocarboxamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04046895 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-c0fd7d00835d4eb89385b596e4113139 |
| Source note | uspto-grants-1977_09 |