HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-{[(2,2-Dichlorocyclopropyl)methyl]sulfanyl}-2-nitroaniline → HCID 20532837, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-{[(2,2-Dichlorocyclopropyl)methyl]sulfanyl}-2-nitroaniline | HCID 20532839 | — |
| Catalyst | Adams' catalyst | HCID 345198 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20532837 | HCID 20532837 | — |
Reaction Steps
A mixture of 8.8 g (0.03 mole) of 4-[(2,2-dichlorocyclopropyl)methyl]thio-2-nitroaniline and 0.6 g of PtO2 in 200 ml of absolute ethanol is reduced on the Parr hydrogenator at 50 psi until the theoretical amount of H2 is absorbed. The mixture is filtered and the solvent is removed in vacuo to yield a dark oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04046908 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-7439281ecbd54d4fa2c5e3e5f497e190 |
| Source note | uspto-grants-1977_09 |