HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride, 3,4-dichloro- → HCID 21409861, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride, 3,4-dichloro- | HCID 76403 | — |
| Reactant | N-Methyl-1-[1-(piperidin-1-yl)cyclohexyl]methanamine | HCID 21409890 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 21409861 | HCID 21409861 | — |
Reaction Steps
Solutions of 1-[1-[(methylamino)methyl]cyclohexyl] piperidine (1.1 g., 0.005 mole) in dry benzene (25 ml) and 3,4-dichlorobenzoyl-chloride (1.0 g., 0.005 mole) in dry benzene (50 ml) were mixed and heated under reflux (steam bath) for 1 hr. The precipitate was filtered washed with benzene and dried. (1. 6 g.) m.p. 222° (dec.)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04049663 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-e0f7b7a397ee4f8db7658706442f6d2c |
| Source note | uspto-grants-1977_09 |