HuagongsheHuagongshe Chemistry Print Report · For research reference only
(Trifluoromethyl)benzene → 3-(Trifluoromethyl)benzenesulfonyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (Trifluoromethyl)benzene | HCID 7368 | — |
| Reactant | Chlorosulfonic acid | HCID 24638 | — |
| Reactant | Fuming sulfuric acid | HCID 24681 | — |
| Product | 3-(Trifluoromethyl)benzenesulfonyl chloride | HCID 2733250 | — |
Reaction Steps
The m-trifluoromethylbenzenesulfonyl chloride starting material was prepared by reacting benzotrifluoride with chlorosulfonic acid in the presence of oleum (65% SO3), according to the method described in Chemical Abstracts 75, 19942d, (1971); German Offen. No. 1,954,448.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04049695 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-9cfa81f884a64a6e97d6763b3e278951 |
| Source note | uspto-grants-1977_09 |