HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → 1-Oxo-2-(2-phenylethanesulfinyl)-1lambda~5~-pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | 1-Oxo-2-[(2-phenylethyl)sulfanyl]-1lambda~5~-pyridine | HCID 13929685 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 1-Oxo-2-(2-phenylethanesulfinyl)-1lambda~5~-pyridine | HCID 53988000 | — |
Reaction Steps
The procedure employed is identical to that of Example 68 using 2.8 gm (0.012 mol) 2-(2-phenylethylthio)pyridine N-oxide in 25 ml of chloroform with 2.4 gm (0.012 mol) MCPBA in 50 ml chloroform.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04050921 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-4f5388de92684f8a926aaff7b61d143b |
| Source note | uspto-grants-1977_09 |