HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorophenol → 2-(4-Chlorophenoxy)propan-1-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorophenol | HCID 4684 | — |
| Reactant | 2-Bromopropan-1-ol | HCID 11713 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | 2-(4-Chlorophenoxy)propan-1-ol | HCID 13259417 | — |
Reaction Steps
2.3 g. of sodium are dissolved in 170 ml. of absolute isopropanol, 12.85 g. of p-chlorophenol are introduced, 13.9 g. of 2-bromo-propanol are added dropwise and the mixture is boiled for 20 hours. The mixture is evaporated and worked up using water and ether to give 2-(4-chlorophenoxy)-propanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04051173 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-ada92a73568243c9addd637e5f2f42ff |
| Source note | uspto-grants-1977_09 |