HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 21408043, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 14119276 | HCID 14119276 | — |
| Reactant | 2-Bromo-2-methylpropan-1-ol | HCID 23458669 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 21408043 | HCID 21408043 | — |
Reaction Steps
A solution of 15.3 g. of 2-bromo-2-methylpropanol in 50 ml. of acetone is added slowly to a stirred mixture consisting of 23.45 g. of 4-p-chlorophenoxymethyl-phenol, 13.8 g. of K2CO3 an 80 ml. of acetone. The mixture is boiled for 12 hours while stirring and then filtered and evaporated to give 2-[4-(4-chlorophenoxymethyl)-phenoxy]-2-methyl-propanol, m.p. 67°-70° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04051173 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-35b3e95274d84250a32ab063e112c69a |
| Source note | uspto-grants-1977_09 |