HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54200407, compound → HCID 54395129, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54200407 | HCID 54200407 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 54395129 | HCID 54395129 | — |
Reaction Steps
Analogously to Example 24, 0.025 mol of 3-amino-5-trifluoromethyl-7-ethoxycarbonylaminoindazole-2-carboxylic acid ethyl ester in 30 ml of dimethylformamide gives 3-amino-5-trifluoromethyl-7-ethoxycarbonylaminoindazole-1-carboxylic acid ethyl ester (melting point: 236°-237° C; 65% of theory) in 1 hour at 155° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04051252 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-17e8ebd013e74400995cb2714a3eb1e4 |
| Source note | uspto-grants-1977_09 |