HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 53681858, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Aminomatacil | HCID 25072 | — |
| Reactant | 1-Propanesulfonyl chloride | HCID 66279 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 53681858 | HCID 53681858 | — |
Reaction Steps
According to the general procedure described in Example 1-C, 3-methyl-4-aminophenyl N-methylcarbamate (4.0g., 0.022 mole) was reacted with n-propanesulfonyl chloride (31.5g., 0.022 mole) and triethylamine (2.47g., 0.024 mole) in benzene. The product (4.0g.) showed the characteristic carbonyl absorption at 5.8μ in the infrared (KBr).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04051254 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-544a6e714a774ab2922b71ec13634c78 |
| Source note | uspto-grants-1977_09 |