Triethylamine → HCID 53681858, compound

HRID 2072424Notes

Reaction equation

HRID 2072424 reaction equation
[CH3:1][NH:2][C:3](=[O:13])[O:4][C:5]1[CH:10]=[CH:9][C:8]([NH2:11])=[C:7]([CH3:12])[CH:6]=1.[CH2:14]([S:17](Cl)(=[O:19])=[O:18])[CH2:15][CH3:16].C(N(CC)CC)C>C1C=CC=CC=1>[CH3:1][NH:2][C:3](=[O:13])[O:4][C:5]1[CH:10]=[CH:9][C:8]([NH:11][S:17]([CH2:14][CH2:15][CH3:16])(=[O:19])=[O:18])=[C:7]([CH3:12])[CH:6]=1

Participants

5

Reactant 3

HCID 8471TriethylamineHCID 25072AminomatacilHCID 662791-Propanesulfonyl chloride

Product 1

HCID 53681858HCID 53681858, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

According to the general procedure described in Example 1-C, 3-methyl-4-aminophenyl N-methylcarbamate (4.0g., 0.022 mole) was reacted with n-propanesulfonyl chloride (31.5g., 0.022 mole) and triethylamine (2.47g., 0.024 mole) in benzene. The product (4.0g.) showed the characteristic carbonyl absorption at 5.8μ in the infrared (KBr).

Workup

  1. customthe characteristic carbonyl absorption at 5.8μ in the

Sources & evidence

ORD record
ord-544a6e714a774ab2922b71ec13634c78
Source dataset
uspto-grants-1977_09
Patent number
US04051254

Reaction notes

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