HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 21409320, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | Aminomatacil | HCID 25072 | — |
| Solvent | Water ethanol | HCID 19096565 | — |
| Product | HCID 21409320 | HCID 21409320 | — |
Reaction Steps
The reaction of 3-methyl-4-aminophenyl N-methylcarbamate (3.6g., 0.02 mole) with ethyl chloroformate (2.28g., 0.021 mole) and triethylamine (2.23g., 0.022 mole) yielded a beige solid (3.6g., m.p. 153°-55° C. from ethanol/water).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04051254 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-2b99f354959244fab559ee0d9cd9b1e5 |
| Source note | uspto-grants-1977_09 |