Triethylamine → HCID 21409320, compound

HRID 2072436Notes

Reaction equation

HRID 2072436 reaction equation
[CH3:1][NH:2][C:3](=[O:13])[O:4][C:5]1[CH:10]=[CH:9][C:8]([NH2:11])=[C:7]([CH3:12])[CH:6]=1.Cl[C:15]([O:17][CH2:18][CH3:19])=[O:16].C(N(CC)CC)C>C(O)C.O>[CH3:1][NH:2][C:3](=[O:13])[O:4][C:5]1[CH:10]=[CH:9][C:8]([NH:11][C:15]([O:17][CH2:18][CH3:19])=[O:16])=[C:7]([CH3:12])[CH:6]=1

Participants

5

Reactant 3

HCID 8471TriethylamineHCID 10928Ethyl chloroformateHCID 25072Aminomatacil

Product 1

HCID 21409320HCID 21409320, compound

Reagents, catalysts & solvents 1

HCID 19096565Water ethanolSolvent

Procedure

The reaction of 3-methyl-4-aminophenyl N-methylcarbamate (3.6g., 0.02 mole) with ethyl chloroformate (2.28g., 0.021 mole) and triethylamine (2.23g., 0.022 mole) yielded a beige solid (3.6g., m.p. 153°-55° C. from ethanol/water).

Sources & evidence

ORD record
ord-2b99f354959244fab559ee0d9cd9b1e5
Source dataset
uspto-grants-1977_09
Patent number
US04051254

Reaction notes

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