HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21409301, compound → HCID 53751002, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21409301 | HCID 21409301 | — |
| Catalyst | Triethylamine | HCID 8471 | — |
| Catalyst | Phenylacetonitrile | HCID 8794 | — |
| Catalyst | Methyl Isocyanate | HCID 12228 | — |
| Product | HCID 53751002 | HCID 53751002 | — |
Reaction Steps
3,5-Dimethyl-4-methoxyacetamidophenol (0.8g., 0.0038 mole, m.p. 169°-73° C., prepared by reaction of methoxyacetyl chloride with 3,5-dimethyl-4-aminophenol) was reacted with methyl isocyanate (0.245g., 0.004 mole) in benzeneacetonitrile using a few drops of triethylamine as a catalyst. After stirring the initially clear reaction solution for about two days, the precipitated product was filtered (0.6g., m.p. 179.5°-82° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04051254 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-ab50a27359bb451184fbf50a48bfaa5d |
| Source note | uspto-grants-1977_09 |