HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 131710917, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 21408245 | HCID 21408245 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 131710917 | HCID 131710917 | 160.6% |
Reaction Steps
8-[(7-Chloro-3,4-dihydro-2-naphthalenyl)methyl]-1-phenyl-1,3,8-triazaspiro[4.5]decan-4-one (1.6 g) is dissolved in 100 ml of absolute ethanol and treated with excess ethereal hydrogen chloride to give the crude hydrochloride salt. The crude salt is crystallized from methanol to yield 1.4 g of the title compound, melting point 274°-275° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04051248 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-d2f5118deb504715951d3eb2be531c3d |
| Source note | uspto-grants-1977_09 |