HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 131710919, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 21408217 | HCID 21408217 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 131710919 | HCID 131710919 | — |
Reaction Steps
8-[(3,4-Dihydro-6,7-dimethyl-2-naphthalenyl)methyl]-1-phenyl-1,3,8-triazaspiro[4.5]decan-4-one (2.1 g) in 100 ml of absolute ethanol is treated with an excess of ethereal hydrogen chloride to yield the crude salt. The title compound (2.1 g) is crystallized from methanol and has a melting point of 276°-277° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04051248 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-72d28be1a3da4fdc89132425c592cb05 |
| Source note | uspto-grants-1977_09 |