Hydrochloric Acid → HCID 131710919, compound

HRID 2072500Notes

Reaction equation

HRID 2072500 reaction equation
[CH3:1][C:2]1[CH:3]=[C:4]2[C:9](=[CH:10][C:11]=1[CH3:12])[CH:8]=[C:7]([CH2:13][N:14]1[CH2:30][CH2:29][C:17]3([N:21]([C:22]4[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=4)[CH2:20][NH:19][C:18]3=[O:28])[CH2:16][CH2:15]1)[CH2:6][CH2:5]2.[ClH:31]>C(O)C>[ClH:31].[CH3:1][C:2]1[CH:3]=[C:4]2[C:9](=[CH:10][C:11]=1[CH3:12])[CH:8]=[C:7]([CH2:13][N:14]1[CH2:30][CH2:29][C:17]3([N:21]([C:22]4[CH:23]=[CH:24][CH:25]=[CH:26][CH:27]=4)[CH2:20][NH:19][C:18]3=[O:28])[CH2:16][CH2:15]1)[CH2:6][CH2:5]2

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 21408217HCID 21408217, compound

Product 1

HCID 131710919HCID 131710919, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

8-[(3,4-Dihydro-6,7-dimethyl-2-naphthalenyl)methyl]-1-phenyl-1,3,8-triazaspiro[4.5]decan-4-one (2.1 g) in 100 ml of absolute ethanol is treated with an excess of ethereal hydrogen chloride to yield the crude salt. The title compound (2.1 g) is crystallized from methanol and has a melting point of 276°-277° C.

Sources & evidence

ORD record
ord-72d28be1a3da4fdc89132425c592cb05
Source dataset
uspto-grants-1977_09
Patent number
US04051248

Reaction notes

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