HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 131710921, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 8-[(1H-Inden-2-yl)methyl]-1-phenyl-1,3,8-triazaspiro[4.5]decan-4-one | HCID 21408198 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 131710921 | HCID 131710921 | — |
Reaction Steps
8-(1H-Inden-2-ylmethyl)-1-phenyl-1,3,8-triazaspiro[4.5]decan-4-one (1.2g) in absolute ethanol (100 ml) is treated with 1.2 equivalents of ethereal hydrogen chloride. Cooling gives the crude hydrochloride salt which is crystallized from absolute ethanol to yield 1.1g of the title compound, melting point 264°-266° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04051248 |
| Source dataset | uspto-grants-1977_09 |
| ORD ID | ord-060f777c1b2c47c0b33aecda80f0a73d |
| Source note | uspto-grants-1977_09 |