HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propargylamine → N-[3-(2,4-Dichlorophenoxy)propyl]prop-2-yn-1-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propargylamine | HCID 239041 | — |
| Reactant | 1-(3-bromopropoxy)-2,4-dichlorobenzene | HCID 249427 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | N-[3-(2,4-Dichlorophenoxy)propyl]prop-2-yn-1-amine | HCID 12738587 | — |
Reaction Steps
2.3 ml of 87% pure 3-(2,4-dichlorophenoxyl) propylbromide (2.99 g; 0.011 mole) and 1.6 ml propargylamine (1.38 g; 0.025 mole) in 30 ml CH3CN and 1.65 g k2CO3 in 3 ml H2O were stirred at room temperature for 5 days.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04913891 |
| Source dataset | uspto-grants-1990_04 |
| ORD ID | ord-7cf97d5e7fe44f1e8bd3165edd7751f9 |
| Source note | uspto-grants-1990_04 |